Phenethylamine → HCID 178427493, compound

HRID 2242159Notes

Reaction equation

HRID 2242159 reaction equation
[CH3:1][C:2]1[CH:6]=[C:5](C)[N:4]([C:8](=[NH:20])[NH:9][S:10]([C:13]2[CH:18]=[CH:17][C:16]([CH3:19])=[CH:15][CH:14]=2)(=[O:12])=[O:11])N=1.CS(O)(=O)=O.[CH2:26](N)[CH2:27][C:28]1C=CC=C[CH:29]=1>>[NH2:20][C:8]([NH:4][CH2:5][CH2:6][C:2]1[CH:1]=[CH:29][CH:28]=[CH:27][CH:26]=1)=[N:9][S:10]([C:13]1[CH:14]=[CH:15][C:16]([CH3:19])=[CH:17][CH:18]=1)(=[O:11])=[O:12]

Participants

4

Reactant 3

HCID 1001PhenethylamineHCID 6395Methanesulfonic AcidHCID 178427489N-[(3,5-dimethylpyrazol-1-yl)-iminomethyl]-4-methylbenzene-sulfonamide

Product 1

HCID 178427493HCID 178427493, compound

Procedure

The compound of Example 14 was prepared according to the accompanying synthesis procedure from 0.5 ml of N-[(3,5-dimethylpyrazol-1-yl)-iminomethyl]-4-methylbenzene-sulfonamide solution (0.2 M, acetonitrile) with 19 mg of methanesulfonic acid and 0.5 ml of phenethylamine solution (1.0 M, acetonitrile) and filed in a substance databank. Calculated mol. wt. 317.41; found mol. wt. (M+H) 318.3; 635.1 (Dimer)

Sources & evidence

ORD record
ord-c0c49d1e9ffd40aeba853197c5e8f570
Source dataset
uspto-grants-2010_03
Patent number
US07671074B2

Reaction notes

Loading…