Methanesulfonic Acid → HCID 67176191, compound

HRID 2242167Notes

Reaction equation

HRID 2242167 reaction equation
[CH3:1][C:2]1[CH:6]=[C:5]([CH3:7])[N:4]([C:8](=[NH:20])[NH:9][S:10]([C:13]2[CH:18]=[CH:17][C:16]([CH3:19])=[CH:15][CH:14]=2)(=[O:12])=[O:11])N=1.CS(O)(=O)=O.[NH2:26]C1C=NC=CC=1>>[NH2:20][C:8]([NH:4][C:5]1[CH:7]=[N:26][CH:1]=[CH:2][CH:6]=1)=[N:9][S:10]([C:13]1[CH:18]=[CH:17][C:16]([CH3:19])=[CH:15][CH:14]=1)(=[O:12])=[O:11]

Participants

4

Reactant 3

HCID 6395Methanesulfonic AcidHCID 100093-AminopyridineHCID 178427489N-[(3,5-dimethylpyrazol-1-yl)-iminomethyl]-4-methylbenzene-sulfonamide

Product 1

HCID 67176191HCID 67176191, compound

Procedure

The compound of Example 24 was prepared according to the accompanying synthesis procedure from 0.5 ml of N-[(3,5-dimethylpyrazol-1-yl)-iminomethyl]-4-methylbenzene-sulfonamide solution (0.2 M, acetonitrile) with 19 mg of methanesulfonic acid and 0.5 ml of 3-aminopyridine solution (1.0 M, acetonitrile) and filed in a substance databank. Calculated mol. wt. 290.34; found mol. wt. (M+H) 291.1; 580.9 (Dimer)

Sources & evidence

ORD record
ord-fab15770960544cba0b6ef6fd4251db7
Source dataset
uspto-grants-2010_03
Patent number
US07671074B2

Reaction notes

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