Phenethylamine → HCID 19937606, compound

HRID 2245337Notes

Reaction equation

HRID 2245337 reaction equation
[C:1]1([CH2:7][CH2:8][NH2:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:10]([O:12][C:13](=[O:16])[CH:14]=[CH2:15])[CH3:11]>CCO>[CH2:10]([O:12][C:13](=[O:16])[CH2:14][CH2:15][NH:9][CH2:8][CH2:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)[CH3:11]

Participants

4

Reactant 2

HCID 1001PhenethylamineHCID 8821Ethyl Acrylate

Product 1

HCID 19937606HCID 19937606, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Phenylethyl amine (10 g) was dissolved in EtOH (50 ml) and then treated with acrylic acid ethyl ester (8.3 g) dropwise under argon at RT. The resulting mixture was allowed to stir over night and was evaporated and dried in vacuo. The residue (18.9 g) was used without further purification. Colorless liquid, MS (ESI): 222.3 (MH+).

Workup

  1. customwas evaporated
  2. customdried in vacuo
  3. customThe residue (18.9 g) was used without further purification

Sources & evidence

ORD record
ord-f47bb1c698584548953b0a266c6992f2
Source dataset
uspto-grants-2010_03
Patent number
US07683079B2

Reaction notes

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