huagongshe.com
HRID224585

反应详情

EQUATION

反应方程式

HRID 224585 的结构方程式

REACTANTS

反应物

1
结构：Cn1c(=O)c(N)c(N)n(-c2ccccc2)c1=O
HCID11075275

未命名化合物

PRODUCTS

生成物

1
结构：CCCc1nc2c([nH]1)c(=O)n(C)c(=O)n2-c1ccccc1
HCID23331678

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCC(=O)OC(=O)CCC
溶剂HCID7798

Butanoic anhydride

C8H14O3

PROCEDURE

实验过程

A solution of 3 g of 5,6-diamino-3-methyl-1-phenyl-2,4-(1H, 3H)-pyrimidinedione XVIII in 25 ml of butyric anhydride was refluxed for 16 hours. After cooling, grey crystals were filtered off and recrystallized from 100 ml of ethanol. Yield 1.1 g NMR.

WORKUP

后处理

  1. temperatureAfter cooling
  2. filtrationgrey crystals were filtered off
  3. customrecrystallized from 100 ml of ethanol