HRID2246240

反应详情

EQUATION

反应方程式

HRID 2246240 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a stirred solution of the product from Step B (1.54 g) in ethyl acetate (30 mL) was added 5% palladium on carbon (298 mg). The reaction mixture was stirred under hydrogen (1 atm) at room temperature for 2 h, then filtered through a pad of Celite and concentrated to give the desired product.

WORKUP

后处理

  1. filtrationfiltered through a pad of Celite
  2. concentrationconcentrated