HRID22480

反应详情

EQUATION

反应方程式

HRID 22480 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

In a manner similar to Example 1, a reaction was conducted using 2-(5-amino-1,2,4-thiadiazol-3-yl)-2-(Z)-methoxyiminoacetic acid whose average particle size was 2.4 μ. Subsequent to dropwise addition of a chlorinating reagent which had been prepared from phosphorus oxychloride and N,N-dimethylformamide, they were reacted for 1 minute. The reaction product was post-treated, and its purity was analyzed by HPLC by the method described above.

WORKUP

后处理

  1. additionSubsequent to dropwise addition of a chlorinating reagent which
  2. customwere reacted for 1 minute
  3. additionThe reaction product was post-treated