huagongshe.com
HRID2249140

反应详情

EQUATION

反应方程式

HRID 2249140 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：CC(C)C1OCC(C(=O)Cl)CO1
HCID17882217

2-(Propan-2-yl)-1,3-dioxane-5-carbonyl chloride

C8H13ClO3

结构：Nc1cc(C(=O)NCCO)cc([N+](=O)[O-])c1
HCID19825445

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)C1OCC(C(=O)Nc2cc(C(=O)NCCO)cc([N+](=O)[O-])c2)CO1
HCID53898412

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)N(C)C
溶剂HCID31374

Dimethylacetamide

C4H9NO

PROCEDURE

实验过程

40 g (0.177 mole) of 3-nitro-5-amino-N-(2-hydroxyethyl)benzamide are dissolved in 400 cm3 of DMAC. The addition of 74.9 g (0.389 mole) of 2-isopropyl-1,3-dioxane-5-carboxylic acid chloride in the presence of triethylamine (54.6 cm3) gives rise to an exothermic reaction.

WORKUP

后处理

  1. customgives rise
  2. customto an exothermic reaction