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HRID2249710

反应详情

EQUATION

反应方程式

HRID 2249710 的结构方程式

REACTANTS

反应物

2
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：CC(=O)N1c2c(ccn3c(C)c(C)nc23)[C@@H](O)[C@H](O)[C@H]1c1ccccc1
HCID69288589

未命名化合物

PRODUCTS

生成物

1
结构：Cc1nc2c3c(ccn2c1C)[C@@H](O)[C@H](O)[C@@H](c1ccccc1)N3
HCID10215014

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：NCCO
溶剂HCID700

Ethanolamine

C2H7NO

PROCEDURE

实验过程

The N-acetyl protecting group is detached from the compound (7R,8R,9R)-10-acetyl-7,8-dihydroxy-2,3-dimethyl-9-phenyl-7,8,9,10-tetrahydroimidazo[1,2-h][1,7]naphthyridine by heating with potassium carbonate in 2-aminoethanol (temp. 70-100° C.). After extractive workup and crystallization, the title compound is obtained as a colourless solid of m.p. 206-209° C.

WORKUP

后处理

  1. customAfter extractive workup and crystallization