Diethylene Glycol Monoethyl Ether → 4-(Acetylamino)benzamide

HRID 225202Notes

Reaction equation

HRID 225202 reaction equation
[Na+].[Na+].P(O[CH2:8][C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O)([O-])([O-])=O.C1N=C(N)C2N=CN([C@@H]3O[C@H](COP(OP(OC[C@H]4[O:48][C@@H:47]([N:49]5[CH:54]=[C:53]([C:55]([NH2:57])=[O:56])[CH2:52][CH:51]=[CH:50]5)[C@H:46](O)[C@@H]4O)(O)=O)(O)=O)[C@@H](O)[C@H]3O)C=2N=1.CCOCCOCCO>C(O)C(N)(CO)CO.Cl>[C:47]([NH:49][C:50]1[CH:51]=[CH:52][C:53]([C:55]([NH2:57])=[O:56])=[CH:54][CH:8]=1)(=[O:48])[CH3:46]

Participants

5

Reactant 3

HCID 8146Diethylene Glycol Monoethyl EtherHCID 439153NadhHCID 18594434d-glucose 6-phosphate disodium salt

Product 1

HCID 5777274-(Acetylamino)benzamide

Reagents, catalysts & solvents 1

HCID 93573Tromethamine hydrochlorideSolvent

Procedure

The following components were combined at a temperature between 0°-4°: G6PDH, 10.0 ml of ca. 2 mg/ml solution suspended in 0.055 M Tris-HCl buffer; Glucose-6-phosphate disodium salt, 100 mg; NADH, 200 mg; Carbitol, 3.0 ml.

Workup

  1. customwere combined at a temperature between 0°-4°

Sources & evidence

ORD record
ord-42cde77fd8844902a5b880c1730b8794
Source dataset
uspto-grants-1980_11
Patent number
US04235969

Reaction notes

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