Triethylamine → HCID 19738053, compound

HRID 2255379Notes

Reaction equation

HRID 2255379 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][C:12]([O:14][CH3:15])=[O:13].[CH3:16][CH:17]1[O:22][CH:21]([CH3:23])[CH2:20][NH:19][CH2:18]1.C(N(CC)CC)C>C1(C)C=CC=CC=1>[CH3:23][CH:21]1[O:22][CH:17]([CH3:16])[CH2:18][N:19]([CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][C:12]([O:14][CH3:15])=[O:13])[CH2:20]1

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 1108622,6-DimethylmorpholineHCID 223913Methyl 11-bromoundecanoate

Product 1

HCID 19738053HCID 19738053, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

This intermediate (12.0 g.) was prepared using the procedure described in Example 4a except using 12 g. (0.045 mole) of methyl 11-bromoundecylate, 5.5 ml. (0.045 mole) of 2,6-dimethylmorpholine, 6.12 ml. of triethylamine, and 15 ml. of toluene and was isolated as a yellow, viscous liquid.

Workup

  1. customThis intermediate (12.0 g.) was prepared

Sources & evidence

ORD record
ord-657051a1ae084f62b86c942dd3f6e903
Source dataset
uspto-grants-1993_08
Patent number
US05240925

Reaction notes

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