Hydrochloric Acid → HCID 22922209, compound

HRID 2258509Notes

Reaction equation

HRID 2258509 reaction equation
[N:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[C:11]1[O:12][C:13]2[CH:19]=[CH:18][C:17]([C:20]([NH:22][S:23]([C:26]3[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=3[CH3:32])(=[O:25])=[O:24])=[O:21])=[CH:16][C:14]=2[CH:15]=1.[ClH:33]>C(OCC)(=O)C>[ClH:33].[N:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[C:11]1[O:12][C:13]2[CH:19]=[CH:18][C:17]([C:20]([NH:22][S:23]([C:26]3[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=3[CH3:32])(=[O:24])=[O:25])=[O:21])=[CH:16][C:14]=2[CH:15]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 22922144HCID 22922144, compound

Product 1

HCID 22922209HCID 22922209, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent2×

Procedure

To a solution of N-[2-(2-quinolyl)benzofuran-5-ylcarbonyl]-2-methylbenzenesulfonamide (0.25 g) in ethyl acetate (100 ml) was added saturated hydrogen chloride in ethyl acetate. The resulting precipitates were collected by filtration and washed with ethyl acetate and ethanol to give N-[2-(2-quinolyl)benzofuran-5-ylcarbonyl]-2-methyl-benzenesulfonamide hydrochloride (0.19 g).

Workup

  1. customThe resulting precipitates
  2. filtrationwere collected by filtration
  3. washwashed with ethyl acetate and ethanol

Sources & evidence

ORD record
ord-d8ff3ae939234306952919d8e5a975f0
Source dataset
uspto-grants-1997_08
Patent number
US05661159

Reaction notes

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