Methyl Acrylate → HCID 23112262, compound

HRID 2264325Notes

Reaction equation

HRID 2264325 reaction equation
[N+:1]([C:4]1[CH:11]=[C:10]([N+:12]([O-:14])=[O:13])[CH:9]=[CH:8][C:5]=1[CH:6]=[O:7])([O-:3])=[O:2].[C:15]([O:19][CH3:20])(=[O:18])[CH:16]=[CH2:17].C1N2CCN(CC2)C1>O1CCOCC1.O>[N+:1]([C:4]1[CH:11]=[C:10]([N+:12]([O-:14])=[O:13])[CH:9]=[CH:8][C:5]=1[CH:6]([OH:7])[C:16](=[CH2:17])[C:15]([O:19][CH3:20])=[O:18])([O-:3])=[O:2]

Participants

6

Reactant 3

HCID 7294Methyl AcrylateHCID 9237DabcoHCID 682502,4-Dinitrobenzaldehyde

Product 1

HCID 23112262HCID 23112262, compound

Reagents, catalysts & solvents 2

HCID 962WaterSolventHCID 312751,4-DioxaneSolvent

Procedure

2,4-Dinitrobenzaldehyde was dissolved in dioxane and water, methyl acrylate and triethylenediamine were added thereto at room temperature, and the whole was stirred to obtain methyl 2-[(2,4-dinitrophenyl) (hydroxy)methyl]acrylate.

Sources & evidence

ORD record
ord-36d04ba3abc9448db4b3a352264bfbf3
Source dataset
uspto-grants-2010_12
Patent number
US07855198B2

Reaction notes

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