HRID2267680

反应详情

EQUATION

反应方程式

HRID 2267680 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The tert-butyl ester 9 (2 g, 6.14 mmol) is suspended in 10 ml of dioxane. DCM is then added until the solid dissolved. To this mixture, 4M-HCl in dioxane (12.3 ml, 49.2 mmol) is added. After stirring over night the solvents are evaporated to leave a white solid product.

WORKUP

后处理

  1. dissolutiondissolved
  2. customare evaporated
  3. customto leave a white solid product