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HRID2267716

反应详情

EQUATION

反应方程式

HRID 2267716 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

2 次

结构：CC(C)(C)OC(=O)NC1CCN(C[C@@H]2CCCN3CCCC[C@H]23)CC1
HCID59600141

未命名化合物

PRODUCTS

生成物

1
结构：Cl.Cl.Cl.NC1CCN(C[C@@H]2CCCN3CCCC[C@H]23)CC1
HCID66841583

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

2 次

PROCEDURE

实验过程

The ester 62 (3.8 g, 10.8 mmol) is dissolved in 15 ml of dioxane and after addition of 70 ml of a 4M solution of HCl in dn of HCl in dioxan the mixture is stirred for 4 hours at RT. The product is filtered off and is used in the next step without further purification.

WORKUP

后处理

  1. filtrationThe product is filtered off
  2. customis used in the next step without further purification