HRID2267868

反应详情

EQUATION

反应方程式

HRID 2267868 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

134 (1.3 g, 3.82 mmol) is dissolved in 250 ml of ethyl acetate and, after addition of Pd—C (200 mg), the mixture is hydrogenated at room temperature for 3 hours. The mixture is filtrated over celite to remove the catalyst and evaporated.

WORKUP

后处理

  1. filtrationThe mixture is filtrated over celite
  2. customto remove the catalyst
  3. customevaporated