HRID2269411

反应详情

EQUATION

反应方程式

HRID 2269411 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

In a similar manner to that described in Example (1a), 4-methoxy-3′-nitrobenzophenone (500 mg), 4-(1-aminoethyl)phenyl acetate hydrochloride (1.0 g), triethylamine (1.63 ml), titanium tetrachloride (0.26 ml), sodium cyanoborohydride (543 mg) and acetic acid (0.17 ml) were reacted, to afford the title compound (215 mg) as a yellow oil.

WORKUP

后处理

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