Chloroform → HCID 68407956, compound

HRID 2271217Notes

Reaction equation

HRID 2271217 reaction equation
C(Cl)(Cl)Cl.CC(N=NC(C#N)(C)C)(C#N)C.[CH:17]([C:19]1[CH:26]=[CH:25][C:22]([CH2:23][Cl:24])=[CH:21][CH:20]=1)=[CH2:18]>CC(C)=O.C=CC1C=CC=CC=1>[CH:17]([C:19]1[CH:26]=[CH:25][C:22]([CH2:23][Cl:24])=[CH:21][CH:20]=1)=[CH2:18].[CH2:18]=[CH:17][C:19]1[CH:26]=[CH:25][CH:22]=[CH:21][CH:20]=1

Participants

6

Reactant 3

HCID 6212ChloroformHCID 6547AzobisisobutyronitrileHCID 74126p-Vinylbenzyl chloride

Product 1

HCID 68407956HCID 68407956, compound

Reagents, catalysts & solvents 2

HCID 180AcetoneSolventHCID 7501StyreneSolvent

Procedure

In a 250 mL three-neck round-bottom flask were placed 90 mL of chloroform, 10 mL of 0.20 M AIBN in acetone, 9.0 mL of styrene (inhibitor removed), and 1.0 mL of p-vinylbenzyl chloride. The mixture was refluxed for 24 h. At the conclusion of the reaction, the solution was cooled and the solvent was removed on a rotary evaporator and the sample was dried in a vacuum oven at 90° C. for 2 h.

Workup

  1. customIn a 250 mL three-neck round-bottom flask were placed
  2. temperatureThe mixture was refluxed for 24 h
  3. customAt the conclusion of the reaction
  4. temperaturethe solution was cooled
  5. customthe solvent was removed on a rotary evaporator
  6. customthe sample was dried in a vacuum oven at 90° C. for 2 h.

Sources & evidence

ORD record
ord-9e3e9b70654b44daa07f6280444755d9
Source dataset
uspto-grants-2001_12
Patent number
US06333385B1

Reaction notes

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