huagongshe.com
HRID2276872

反应详情

EQUATION

反应方程式

HRID 2276872 的结构方程式

REACTANTS

反应物

3
结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：O=C(NC1N=C(c2ccccc2)c2ccccc2NC1=O)OCc1ccccc1
HCID2756242

未命名化合物

结构：Clc1ccc(I)nc1
HCID11118148

5-Chloro-2-iodopyridine

C5H3ClIN

PRODUCTS

生成物

1
结构：N[C@H]1N=C(c2ccccc2)c2ccccc2N(c2ccc(Cl)cn2)C1=O
HCID90080293

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO.O
溶剂HCID22242641

Methanol--water (1/1)

CH6O2

PROCEDURE

实验过程

Intermediate B-16 was prepared from benzyl 2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylcarbamate and 5-chloro-2-iodopyridine according to the procedure described for Intermediate B-15. RT=2.430 min (H2O/CH3OH with TFA, CHROMOLITH® ODS S5 4.6×50 mm, gradient=3 min, wavelength=220 and 254 nm); MS(ES):m/z=363.12 [M+H+].