Gamma-Butyrolactone → HCID 20542962, compound

HRID 2285946Notes

Reaction equation

[CH2:1]([CH:3]([CH2:6][CH2:7][CH2:8][CH3:9])[CH2:4][NH2:5])[CH3:2].[C:10]1(=[O:15])[O:14][CH2:13][CH2:12][CH2:11]1>>[CH2:1]([CH:3]([CH2:6][CH2:7][CH2:8][CH3:9])[CH2:4][NH:5][C:13](=[O:14])[CH2:12][CH2:11][CH2:10][OH:15])[CH3:2]

Participants

Reactant 2

HCID 7302Gamma-Butyrolactone

HCID 77192-Ethylhexylamine

Product 1

HCID 20542962HCID 20542962, compound

Conditions

Temperature: 100 °C

Procedure

In a glass reaction vessel 12.9 grams of 2-ethylhexylamine were admixed with 8.6 grams of butyrolactone and the mixture heated to 100° C. on a steam bath until reaction was completed in a period of one hour. A conversion of greater than 95%, based on butyrolactone, was achieved. The product upon cooling to room temperature was a colorless, clear, moderately viscous liquid. IR=6.09 mu.

Workup

temperatureThe product upon cooling to room temperature

Sources & evidence

ORD record: ord-a21bdab277894ad68bc57240b693733e
Source dataset: uspto-grants-1982_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04325973

Reaction notes

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