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HRID2286405

反应详情

EQUATION

反应方程式

HRID 2286405 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)Br
HCID10482

Acetyl bromide

C2H3BrO

结构：COc1c(O)cc2c(c1Sc1ccccc1)CCN(C)CC2
HCID23462859

未命名化合物

PRODUCTS

生成物

1
结构：COc1c(OC(C)=O)cc2c(c1Sc1ccccc1)CCN(C)CC2
HCID23462857

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O=C(O)C(F)(F)F
溶剂HCID6422

未命名化合物

PROCEDURE

实验过程

Reaction of 8-hydroxy-7-methoxy-3-methyl-6-phenylthio-2,3,4,5-tetrahydro-1H-3-benzazepine with acetyl bromide in trifluoroacetic acid gave 8-acetoxy-7-methoxy-3-methyl-6-phenylthio-2,3,4,5-tetrahydro-1H-3-benzazepine; hydrochloride salt m.p. 240°-241° C.