Dodecanoyl chloride → HCID 15521540, compound

HRID 2287918Notes

Reaction equation

HRID 2287918 reaction equation
[NH:1]1[CH2:5][CH2:4][NH:3][C:2]1=[O:6].C(N(CC)CC)C.[C:14](Cl)(=[O:26])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25]>C1(C)C=CC=CC=1>[C:14]([N:1]1[CH2:5][CH2:4][NH:3][C:2]1=[O:6])(=[O:26])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25]

Participants

5

Reactant 3

HCID 8166Dodecanoyl chlorideHCID 84532-ImidazolidinoneHCID 8471Triethylamine

Product 1

HCID 15521540HCID 15521540, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent2×

Procedure

To a solution of 2-imidazolidone in toluene with an appropriate base (e.g., triethylamine) is added a solution of an equimolar amount of lauroyl chloride in toluene. This is stirred overnight, filtered and the filtrate concentrated to give the above product.

Workup

  1. filtrationfiltered
  2. concentrationthe filtrate concentrated
  3. customto give the above product

Sources & evidence

ORD record
ord-8dcf0e3ce9a142f8a55c410dd7b530a4
Source dataset
uspto-grants-2000_07
Patent number
US06086905

Reaction notes

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