p-Toluenesulfonic acid → HCID 4370247, compound

HRID 2292403Notes

Reaction equation

[CH2:1]([CH:7]([CH2:10][OH:11])[CH2:8][OH:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[Br:12][C:13]1[CH:20]=[CH:19][C:16]([CH:17]=O)=[CH:15][CH:14]=1.C1(C)C=CC(S(O)(=O)=O)=CC=1>>[Br:12][C:13]1[CH:20]=[CH:19][C:16]([CH:17]2[O:9][CH2:8][CH:7]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH3:6])[CH2:10][O:11]2)=[CH:15][CH:14]=1

Participants

Reactant 3

HCID 6101p-Toluenesulfonic acid

HCID 707414-Bromobenzaldehyde

HCID 2684842-Hexylpropane-1,3-diol

Product 1

HCID 4370247HCID 4370247, compound

Procedure

Quantities: compound from Example 7 (44 g, 0.27 mol), 4-bromobenzaldehyde (49 g, 0.27 mol) and 4-toluenesulphonic acid (150 mg). The experimental procedure was as described in Example 11.

Sources & evidence

ORD record: ord-257dd8066f694ad087194fcbdc1ff55d
Source dataset: uspto-grants-1997_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05683623

Reaction notes

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