4-Bromophenol → 1-(4-Bromophenoxy)heptane

HRID 2292438Notes

Reaction equation

HRID 2292438 reaction equation
C(=O)([O-])[O-].[K+].[K+].Br[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[Br:15][C:16]1[CH:21]=[CH:20][C:19]([OH:22])=[CH:18][CH:17]=1>>[Br:15][C:16]1[CH:21]=[CH:20][C:19]([O:22][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14])=[CH:18][CH:17]=1

Participants

4

Reactant 3

HCID 78084-BromophenolHCID 11430Potassium CarbonateHCID 123691-Bromoheptane

Product 1

HCID 5991021-(4-Bromophenoxy)heptane

Procedure

Quantities: anhydrous potassium carbonate (34.8 g, 0.25 mol), 1-bromoheptane (19.6 g, 0.11 mol) and 4-bromophenol (17.3 g, 0.1 mol). The experimental procedure was as described in Example 119.

Sources & evidence

ORD record
ord-669f60a2b3cf4e9d8e1a2770f8d8208b
Source dataset
uspto-grants-1997_11
Patent number
US05683623

Reaction notes

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