Phenethylamine → 113721-77-0

HRID 2293128Notes

Reaction equation

[CH2:1]([NH2:9])[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[F:10][C:11]([F:16])([F:15])[C:12](O)=O>>[F:10][C:11]([F:16])([F:15])[CH:12]1[C:8]2[C:3](=[CH:4][CH:5]=[CH:6][CH:7]=2)[CH2:2][CH2:1][NH:9]1

Participants

Reactant 2

HCID 1001Phenethylamine

HCID 6422Trifluoroacetic acid

Product 1

HCID 21476433113721-77-0

Procedure

In accordance with the same procedures as in Preparation 1-1, except that 25 ml of phenethylamine(0.2M) and 30 ml of anhydrous trifluoroacetic acid(0.21M) were used as starting materials, 5.4 g of the title compound was prepared.

Workup

customIn accordance with the same procedures as in Preparation 1-1

Sources & evidence

ORD record: ord-ab1c1ac0229842e992968e8bb7a17d5b
Source dataset: uspto-grants-1997_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05686458

Reaction notes

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