N-Methylaniline → HCID 70197756, compound

HRID 2293143Notes

Reaction equation

HRID 2293143 reaction equation
[Cl:1][C:2]1[N:11]=[C:10]([N:12]2[CH2:21][CH2:20][C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[CH:13]2[CH3:22])[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[N:3]=1.[CH3:23][NH:24][C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1>CN(C)C=O>[ClH:1].[CH3:23][N:24]([C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1)[C:2]1[N:11]=[C:10]([N:12]2[CH2:21][CH2:20][C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[CH:13]2[CH3:22])[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[N:3]=1

Participants

4

Reactant 2

HCID 7515N-MethylanilineHCID 21476447HCID 21476447, compound

Product 1

HCID 70197756HCID 70197756, compoundYield 54%

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

In accordance with the same procedures as in Example 18, except that to a mixture of 1.4 g of the compound (4.52 mM) prepared in Example 2 and 15 ml of dimethyl-formamide, 1.1 ml of N-methylaniline(10.1 mM) was added, 1.02 g of the title compound was prepared.

Workup

  1. additionwas added

Sources & evidence

ORD record
ord-66c76a647b684bf8859369bb67912823
Source dataset
uspto-grants-1997_11
Patent number
US05686458

Reaction notes

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