N-Methylaniline → HCID 70195076, compound

HRID 2293156Notes

Reaction equation

HRID 2293156 reaction equation
[Cl:1][C:2]1[N:11]=[C:10]([N:12]2[CH2:21][CH2:20][C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[CH:13]2[CH3:22])[C:9]2[C:4](=[C:5]([O:23][CH3:24])[CH:6]=[CH:7][CH:8]=2)[N:3]=1.[CH3:25][NH:26][C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1>CN(C)C=O>[ClH:1].[CH3:24][O:23][C:5]1[CH:6]=[CH:7][CH:8]=[C:9]2[C:4]=1[N:3]=[C:2]([N:26]([C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1)[CH3:25])[N:11]=[C:10]2[N:12]1[CH2:21][CH2:20][C:19]2[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=2)[CH:13]1[CH3:22]

Participants

4

Reactant 2

HCID 7515N-MethylanilineHCID 21476458HCID 21476458, compound

Product 1

HCID 70195076HCID 70195076, compoundYield 22%

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

In accordance with the same procedures as in Example 18, except that to a mixture of 8.00 g of the compound (8.82 mM) prepared in Example 5 and 15 ml of dimethyl-formamide, 2.00 ml of N-methyl aniline(18.45 mM) was added, 0.85 g of the title compound was prepared.

Workup

  1. additionwas added

Sources & evidence

ORD record
ord-a1f2be8c1d8f483a9ef29846a029b170
Source dataset
uspto-grants-1997_11
Patent number
US05686458

Reaction notes

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