Hydrochloric Acid → HCID 18387085, compound

HRID 2296586Notes

Reaction equation

HRID 2296586 reaction equation
C([O:5][CH:6]([C:22]([OH:24])=[O:23])[N:7]([CH2:17][CH2:18][S:19][CH2:20][CH3:21])[CH:8]([O:12]C(C)(C)C)[C:9]([OH:11])=[O:10])(C)(C)C.[ClH:25]>O1CCCC1>[ClH:25].[OH:5][CH:6]([C:22]([OH:24])=[O:23])[N:7]([CH2:17][CH2:18][S:19][CH2:20][CH3:21])[CH:8]([OH:12])[C:9]([OH:11])=[O:10]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 18387080HCID 18387080, compound

Product 1

HCID 18387085HCID 18387085, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

1.67 g (5 mmol) of N,N-bis-(tert-butoxycarboxy-methyl)-S-ethyl-2-mercaptoethylamine is dissolved in 12 ml of tetrahydrofuran and mixed with 6 ml of concentrated hydrochloric acid. The resulting reaction mixture is stirred for 1 hour at room temperature and concentrated by evaporation in a vacuum. The residue is pulverized with 10 ml of absolute diethyl ether. Then, the product is filtered off and dried in a medium-high vacuum.

Workup

  1. customThe resulting reaction mixture
  2. concentrationconcentrated by evaporation in a vacuum
  3. filtrationThen, the product is filtered off
  4. customdried in a medium-high vacuum

Sources & evidence

ORD record
ord-2f70cfc310794dc78a54f2efdc4ae944
Source dataset
uspto-grants-2002_12
Patent number
US06488909B1

Reaction notes

Loading…