p-Toluenesulfonic acid → HCID 18379757, compound

HRID 2299097Notes

Reaction equation

HRID 2299097 reaction equation
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]([NH2:8])=[O:7].[CH3:9][C:10]([CH:13]=O)([CH3:12])[CH3:11].[NH:15]1[C:19]2[CH:20]=[CH:21][CH:22]=[CH:23][C:18]=2[N:17]=[N:16]1.C1(C)C=CC(S(O)(=O)=O)=CC=1>C1(C)C(C)=CC=CC=1>[N:15]1([CH:13]([NH:8][C:6]([C:2]2[O:1][CH:5]=[CH:4][CH:3]=2)=[O:7])[C:10]([CH3:11])([CH3:12])[CH3:9])[C:19]2[CH:20]=[CH:21][CH:22]=[CH:23][C:18]=2[N:17]=[N:16]1

Participants

6

Reactant 4

HCID 6101p-Toluenesulfonic acidHCID 12417PivalaldehydeHCID 69108FuramideHCID 178418385HCID 178418385, compound

Product 1

HCID 18379757HCID 18379757, compound

Reagents, catalysts & solvents 1

HCID 7237O-XyleneSolvent

Procedure

Furan-2-carboxamide, pivaldehyde, benzotriazole, and p-toluenesulfonic acid in xylene were processed as described in Example 18B to provide the title compound.

Sources & evidence

ORD record
ord-d1c06f72f25048d29e0b92563b5f21ae
Source dataset
uspto-grants-2002_12
Patent number
US06495576B2

Reaction notes

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