HRID2303591

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID24758

Sodium hydride

HNa

HCID15479960

5-Chloro-2-isocyanato-1,3-di(propan-2-yl)benzene

C13H16ClNO

反应SMILES：CC(=O)c1cc(C(C)=O)cc(S(N)(=O)=O)c1

HCID18461608

未命名化合物

PRODUCTS

产物

反应SMILES：CC(=O)c1cc(C(C)=O)cc(S(=O)(=O)NC(=O)Nc2c(C(C)C)cc(Cl)cc2C(C)C)c1

HCID22116283

未命名化合物

收率 40.3%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

The title compound was prepared as described in method A from 3,5-diacetylbenzenesulfonamide (0.35 grams), 4-chloro-2,6-diisopropylphenylisocyanate (0.37 grams), sodium hydride (0.06 grams of a 60% dispersion in mineral oil), in tetrahydrofuran (4 mL). This afforded 0.28 grams of the title compound, m.p. 201.9-203.4° C.

WORKUP

后处理

customThe title compound was prepared