HRID2304601

反应详情

EQUATION

反应方程式

HRID 2304601 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

[4-(4-Methoxyphenyl)-5-(3-pyridyl)-I,3-thiazol-2-yl]amine (200 mg) was dissolved in 1% methanol solution of hydrogen chloride (3.2 mL), and the solvent was evaporated. The crude crystalline was recrystallized from methanol-ethyl acetate to give the title compound (180 mg, yield 80%).

WORKUP

后处理

  1. customthe solvent was evaporated
  2. customThe crude crystalline was recrystallized from methanol-ethyl acetate