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HRID230663

反应详情

EQUATION

反应方程式

HRID 230663 的结构方程式

REACTANTS

反应物

2
结构：CNCc1ccccc1
HCID7669

N-Methylbenzylamine

C8H11N

结构：O=C(O)Cc1ccc(-n2nc(C(F)(F)F)c3c2CCCC3)cc1
HCID50992931

未命名化合物

PRODUCTS

生成物

1
结构：CN(Cc1ccccc1)C(=O)Cc1ccc(-n2nc(C(F)(F)F)c3c2CCCC3)cc1
HCID24827047

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from {4-[3-(trifluoromethyl)-4,5,6,7-tetrahydro-1H-indazol-1-yl]phenyl}acetic acid and N-methylbenzylamine using a similar procedure to that described for Example 13, but purified by flash column chromatography eluting from 0-66% ethyl acetate in hexane.

WORKUP

后处理

  1. custompurified by flash column chromatography
  2. washeluting from 0-66% ethyl acetate in hexane