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HRID2308163

反应详情

EQUATION

反应方程式

HRID 2308163 的结构方程式

REACTANTS

反应物

4
结构：CN(C)C=O
HCID6228

N,N-Dimethylformamide

C3H7NO

结构：O=P(Cl)(Cl)Cl
HCID24813

Phosphoric trichloride

Cl3OP

结构：CCCCCCCn1c2ccc(C=O)cc2c2cc(C=O)ccc21
HCID11141782

N-heptyl-3,6-Diformylcarbazole

C21H23NO2

结构：CCCCCCc1cccc2c3ccccc3n(CC)c12
HCID66872719

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCc1cc(C=O)cc2c3cc(C=O)ccc3n(CC)c12
HCID86590067

未命名化合物

PROCEDURE

实验过程

N-2-ethylhexyl-3,6-diformyl carbazole was prepared from DMF (97 ml, 1.25 mol), POCl3 (116.5 ml, 1.25 mol), and N-2-ethylhexylcarbazole (50 g, 0.18 mol) according to the procedure described for N-Heptyl-3,6-Diformylcarbazole. The product was obtained as 40 g of brownish liquid (66% yield). The product was used as is in the next step without any purification.