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HRID2309221

反应详情

EQUATION

反应方程式

HRID 2309221 的结构方程式

REACTANTS

反应物

3
结构：O
HCID962

Water

H2O

结构：CC[C@H](C)[C@H](N)C1=N[C@H](C(=O)N[C@@H](CC(C)C)C(=O)N[C@H](CCC(=O)O)C(=O)N[C@H](C(=O)N[C@H]2CCCCNC(=O)[C@H](CC(N)=O)NC(=O)[C@@H](CC(=O)O)NC(=O)[C@H](Cc3cnc[nH]3)NC(=O)[C@@H](Cc3ccccc3)NC(=O)[C@H]([C@@H](C)CC)NC(=O)[C@@H](CCCN)NC2=O)[C@@H](C)CC)CS1
HCID10909430

未命名化合物

结构：CC[C@@H](C(=O)[C@@H](C)[C@@H](O)[C@@H](C)[C@H]1O[C@@H](CC(=O)OO)[C@H](C)C[C@@H]1C)[C@H]1O[C@](C)([C@]2(O)O[C@](CC)([C@@H](O)CC)C[C@H]2C)C[C@@H]1C.[Cu]
HCID86741795

未命名化合物

PRODUCTS

生成物

1
结构：CC[C@@H](C(=O)[C@@H](C)[C@@H](O)[C@@H](C)[C@H]1O[C@@H](CC(=O)OO)[C@H](C)C[C@@H]1C)[C@H]1O[C@](C)([C@]2(O)O[C@](CC)([C@@H](O)CC)C[C@H]2C)C[C@@H]1C.CC[C@H](C)[C@H](N)C1=N[C@H](C(=O)N[C@@H](CC(C)C)C(=O)N[C@H](CCC(=O)O)C(=O)N[C@H](C(=O)N[C@H]2CCCCNC(=O)[C@H](CC(N)=O)NC(=O)[C@@H](CC(=O)O)NC(=O)[C@H](Cc3cnc[nH]3)NC(=O)[C@@H](Cc3ccccc3)NC(=O)[C@H]([C@@H](C)CC)NC(=O)[C@@H](CCCN)NC2=O)[C@@H](C)CC)CS1.[Cu]
HCID86741794

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

A solution of 3.0 g of copper lysocellin, prepared as described in Example B above, in 25 ml of methanol was stirred while 2.8 g of bacitracin (reg) was added thereto. The mixture was stirred at room temperature for 1 hour. Water was added slowly to precipitate the complex. The crude complex precipitated as a tacky semi-solid which on continued stirring was recovered as a filterable amorphous solid. The crude product was slurried with ethyl acetate, isolated and dried at 40° C. under 5 millimeters (mm) Hg pressure.

WORKUP

后处理

  1. additionwas added
  2. customto precipitate the complex
  3. customThe crude complex precipitated as a tacky semi-solid which
  4. stirringon continued stirring
  5. customwas recovered as a filterable amorphous solid
  6. customisolated
  7. customdried at 40° C. under 5 millimeters (mm) Hg pressure