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HRID2309222

反应详情

EQUATION

反应方程式

HRID 2309222 的结构方程式

REACTANTS

反应物

3
结构：O
HCID962

Water

H2O

结构：CC[C@H](C)[C@H](N)C1=N[C@H](C(=O)N[C@@H](CC(C)C)C(=O)N[C@H](CCC(=O)O)C(=O)N[C@H](C(=O)N[C@H]2CCCCNC(=O)[C@H](CC(N)=O)NC(=O)[C@@H](CC(=O)O)NC(=O)[C@H](Cc3cnc[nH]3)NC(=O)[C@@H](Cc3ccccc3)NC(=O)[C@H]([C@@H](C)CC)NC(=O)[C@@H](CCCN)NC2=O)[C@@H](C)CC)CS1
HCID10909430

未命名化合物

结构：CC[C@@H](C(=O)[C@@H](C)[C@@H](O)[C@@H](C)[C@H]1O[C@@H](CC(=O)OO)[C@H](C)C[C@@H]1C)[C@H]1O[C@](C)([C@]2(O)O[C@](CC)([C@@H](O)CC)C[C@H]2C)C[C@@H]1C.[Mn]
HCID86741789

未命名化合物

PRODUCTS

生成物

1
结构：CC[C@@H](C(=O)[C@@H](C)[C@@H](O)[C@@H](C)[C@H]1O[C@@H](CC(=O)OO)[C@H](C)C[C@@H]1C)[C@H]1O[C@](C)([C@]2(O)O[C@](CC)([C@@H](O)CC)C[C@H]2C)C[C@@H]1C.CC[C@H](C)[C@H](N)C1=N[C@H](C(=O)N[C@@H](CC(C)C)C(=O)N[C@H](CCC(=O)O)C(=O)N[C@H](C(=O)N[C@H]2CCCCNC(=O)[C@H](CC(N)=O)NC(=O)[C@@H](CC(=O)O)NC(=O)[C@H](Cc3cnc[nH]3)NC(=O)[C@@H](Cc3ccccc3)NC(=O)[C@H]([C@@H](C)CC)NC(=O)[C@@H](CCCN)NC2=O)[C@@H](C)CC)CS1.[Mn]
HCID86741796

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

A solution of 6.5 g of manganese lysocellin, prepared as described in Example D above, in 60 ml of methanol was stirred while 7.0 g bacitracin (reg) was added. The solution was stirred at room temperature for four hours. Stirring was continued and water was added slowly to precipitate a tacky semi-solid. The solids were isolated by decantation and washed with fresh water to obtain a filtrable amorphous solid. The solids were isolated, washed with water and dried. The crude product was slurried with toluene (10 ml/g) to obtain an amorphous product.

WORKUP

后处理

  1. additionwas added
  2. stirringStirring
  3. customto precipitate a tacky semi-solid
  4. customThe solids were isolated by decantation
  5. washwashed with fresh water
  6. customto obtain a filtrable amorphous solid
  7. customThe solids were isolated
  8. washwashed with water
  9. customdried
  10. customto obtain an amorphous product