HRID231753

反应详情

EQUATION

反应方程式

HRID 231753 的结构方程式

PROCEDURE

实验过程

To 160 g of 85% aqueous lactic acid solution was added 38 g of glycolic acid and the mixture was heated in a nitrogen atmosphere under reduced pressure for 6 hours in a manner such that the inside temperature and pressure were initially 105° C. and 350 mmHg, respectively, and finally 150° C. and 30 mmHg, respectively, while removing the water distilled. Heating under reduced pressure was further conducted at 3-5 mmHg and 175° C. for 36 hours. Upon cooling to room temperature, there was obtained a colorless lactic acid-glycolic acid copolymer.

WORKUP

后处理

  1. temperaturethe mixture was heated in a nitrogen atmosphere under reduced pressure for 6 hours in a manner such that the inside temperature and pressure
  2. customwere initially 105° C.
  3. custom350 mmHg, respectively, and finally 150° C. and 30 mmHg, respectively, while removing the water
  4. distillationdistilled
  5. temperatureHeating under reduced pressure