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HRID232673

反应详情

EQUATION

反应方程式

HRID 232673 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(S(=O)(=O)O)cc1
HCID6101

4-Methylbenzenesulfonic acid

C7H8O3S

结构：CCOC(=O)C(C(=O)OCC)C(=O)c1c(F)c(F)c(F)c(F)c1CC
HCID54490655

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)CC(=O)c1c(F)c(F)c(F)c(F)c1CC
HCID53931173

未命名化合物

收率 80.4%

PROCEDURE

实验过程

Employing diethyl 2-ethyl-3,4,5,6-tetrafluoro-benzoylmalonate (17.2 g) and p-toluenesulfonic acid (0.25 g), the procedure of Reference Example 19 is repeated to give ethyl 2-ethyl-3,4,5,6-tetrafluorobenzoylacetate (11.09 g).