HRID232816

反应详情

EQUATION

反应方程式

HRID 232816 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a 30% solution of 2-phenylimidazole (144 g, 1 mole) and 2-naphthol (144 g, 1 mole) in isopropanol, formaline (37% aqueous solution, 1 mole of CH2O) is added over a period of 30 minutes at room temperature, followed by six hours of refluxing at 82°-84° C. The product (270 g of a white powder) is obtained in a yield of 90%.

WORKUP

后处理

  1. temperatureof refluxing at 82°-84° C