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HRID23289

反应详情

EQUATION

反应方程式

HRID 23289 的结构方程式

REACTANTS

反应物

2
结构：O=Cc1ccc(Cl)c(Cl)c1
HCID22710

3,4-Dichlorobenzaldehyde

C7H4Cl2O

结构：CC(C)(C)OC(=O)N1CC[C@H]2[C@@H](C1)c1cc(N)cc3c1N2CCSC3
HCID86586437

未命名化合物

PRODUCTS

生成物

1
结构：Clc1ccc(CNc2cc3c4c(c2)[C@@H]2CNCC[C@@H]2N4CCSC3)cc1Cl
HCID60071820

未命名化合物

PROCEDURE

实验过程

Using 3,4-dichlorobenzaldehyde and following the procedures described in EXAMPLE 126, tert-butyl (7bR,11aS)-6-amino-1,2,7b,10,11,11a-hexahydro-4H-pyrido[4,3-b][1,4]thiazepino[6,5,4-hi]indole-9(8H)-carboxylate from EXAMPLE 33, Part B was converted into the title compound of EXAMPLE 158. LRMS (ES)+: 420.4 (M+H)+.