HRID2351450

反应详情

EQUATION

反应方程式

HRID 2351450 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Prepared analogously to Example 1 from 11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and (-)-2-[2-[(dipropylamino)methyl]-piperidin-l-yl]ethanamine in a yield of 90% of theory. Colourless crystals, m.p. 164°-165° C. (acetonitrile); [α]D20 =-7.62° (dilute aqueous hydrochloric acid).