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HRID23564

反应详情

EQUATION

反应方程式

HRID 23564 的结构方程式

REACTANTS

反应物

4
结构：O
HCID962

Water

H2O

结构：CN(C)C=O
HCID6228

N,N-Dimethylformamide

C3H7NO

结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：NC(=O)c1ccc(Cl)nc1
HCID80456

6-Chloronicotinamide

C6H5ClN2O

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NC1CCN(c2ccc(C(N)=O)cn2)CC1
HCID11484042

未命名化合物

CONDITIONS

反应条件

温度
80 °C

PROCEDURE

实验过程

A mixture of 3 g (0.015 mol) of the product of preparation 1, 1.5 g (0.015 mol) of triethylamine and 2.34 g (0.015 mol) of 6-chloronicotinamide in 60 ml of dimethylformamide is heated at 80° C. for 18 hours. After cooling, water is added and the product is filtered off. 2.8 g of the title compound are thus obtained. m.p. 255° C. dec.

WORKUP

后处理

  1. temperatureAfter cooling
  2. filtrationthe product is filtered off