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HRID2356610

反应详情

EQUATION

反应方程式

HRID 2356610 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：Oc1ccc(Cl)cc1I
HCID620234

4-Chloro-2-iodophenol

C6H4ClIO

结构：Fc1cc(Cl)ccc1CBr
HCID2736551

1-(bromomethyl)-4-chloro-2-fluorobenzene

C7H5BrClF

PRODUCTS

生成物

1
结构：Fc1cc(Cl)ccc1COc1ccc(Cl)cc1I
HCID24753687

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

As for Reaction 1, using 84.87 g 4-chloro-2-iodophenol, 76 g 4-chloro-2-fluorobenzyl bromide and 92 g potassium carbonate in 900 ml acetone. Yield 129.36 g. Identical by TLC with product of Reaction 1.

WORKUP

后处理

  1. customAs for Reaction 1
  2. customIdentical by TLC with product of Reaction 1