反应详情

A mixture of about 527 mg of 1-[2-methoxy-3-(triphenylmethoxy)propoxy]-4-tetradecylbenzene, about 10 mg of p-toluenesulfonic acid and about 5 ml of methanol:tetrahydrofuran (about 1:1) was stirred under argon for about 16 hours and the solvents removed under reduced pressure. The residue was dissolved in ether:hexane (about 1:1), washed with aqueous sodium bicarbonate, brine, dried and evaporated, giving about 171 mg of the desired title compound, mp 43°-45° C.

1. customthe solvents removed under reduced pressure
2. dissolutionThe residue was dissolved in ether
3. washhexane (about 1:1), washed with aqueous sodium bicarbonate, brine
4. customdried
5. customevaporated