2-Chlorobenzaldehyde → HCID 58000837, compound

HRID 2358260Notes

Reaction equation

HRID 2358260 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=O)[C:9]([C:12]2C=C[N:15]=[C:14](F)[CH:13]=2)=[N:10][OH:11])=[CH:4][CH:3]=1.[Cl:20][C:21]1[CH:28]=[CH:27][CH:26]=[CH:25][C:22]=1[CH:23]=O.[C:29]([O-:32])(=O)[CH3:30].[NH4+:33]>C(O)(=O)C>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[N:33]=[C:23]([C:22]3[CH:25]=[CH:26][CH:27]=[CH:28][C:21]=3[Cl:20])[N:10]([OH:11])[C:9]=2[C:12]2[CH:13]=[CH:14][NH:15][C:29](=[O:32])[CH:30]=2)=[CH:4][CH:3]=1

Participants

5

Reactant 3

HCID 69962-ChlorobenzaldehydeHCID 517165Ammonium AcetateHCID 136355272HCID 136355272, compound

Product 1

HCID 58000837HCID 58000837, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

Using the general procedure found in Example 1 Step C, the intermediate from Example 1 Step B was combined with 2-chlorobenzaldehyde, ammonium acetate and acetic acid.

Sources & evidence

ORD record
ord-a9f60e06aea34199980ca41226e24e55
Source dataset
uspto-grants-2010_07
Patent number
US07763634B2

Reaction notes

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