Hydrogen Peroxide → HCID 178424958, compound

HRID 2361450Notes

Reaction equation

HRID 2361450 reaction equation
[CH3:1][C:2]1([CH3:11])[N:7]([O:8])[C:6]([CH3:10])([CH3:9])[CH2:5][CH2:4][CH2:3]1.[Br-].[Na+].[OH:14][OH:15]>O>[CH3:9][C:6]1([CH3:10])[N:7]([O:8])[C:2]([CH3:11])([CH3:1])[CH2:3][CH2:4][CH2:5]1.[OH:14][OH:15]

Participants

5

Reactant 3

HCID 784Hydrogen PeroxideHCID 253881Sodium BromideHCID 2724126Tempo

Product 1

HCID 178424958HCID 178424958, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A sample of cotton textile (ca. 1 g) is added to a solution composed of 90 mL water with 10 mg (0.065 mmol) TEMPO and 0.22 g (2 mmol) sodium bromide. Hydrogen peroxide 3% is added (0.9 mL, 1 mmol) and the reaction stirred at RT for 10 minutes to 2 hours. The material is washed with water, dried, and used without further modification in the following ZnO deposition step.

Workup

  1. additionA sample of cotton textile (ca. 1 g) is added to a solution
  2. washThe material is washed with water
  3. customdried

Sources & evidence

ORD record
ord-4e6eefc1385d45b4936b6f6d7c5df5e2
Source dataset
uspto-grants-2014_04
Patent number
US08690964B2

Reaction notes

Loading…