Methylamine → HCID 19921522, compound

HRID 2368656Notes

Reaction equation

HRID 2368656 reaction equation
Cl[C:2]1[C:10]([N+:11]([O-:13])=[O:12])=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][N:3]=1.[CH3:14][NH2:15]>C1COCC1>[CH3:14][NH:15][C:2]1[C:10]([N+:11]([O-:13])=[O:12])=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][N:3]=1

Participants

4

Reactant 2

HCID 6329MethylamineHCID 3464596-CHLORO-5-NITRONICOTINIC ACID

Product 1

HCID 19921522HCID 19921522, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

Prepared analogously to example 154a from 6-chloro-5-nitro-nicotinic acid and 2 M methylamine solution in THF.

Sources & evidence

ORD record
ord-c3840bba10d44421bc04015c55564ec1
Source dataset
uspto-grants-2014_04
Patent number
US08703796B2

Reaction notes

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