Proxicromil → HCID 23668092, compound

HRID 236953Notes

Reaction equation

HRID 236953 reaction equation
[OH:1][C:2]1[C:15]2[C:14](=[O:16])[CH:13]=[C:12]([C:17]([OH:19])=[O:18])[O:11][C:10]=2[C:9]([CH2:20][CH2:21][CH3:22])=[C:8]2[C:3]=1[CH2:4][CH2:5][CH2:6][CH2:7]2.C(=O)(O)[O-].[Na+:27].[Na]>O>[OH:1][C:2]1[C:15]2[C:14](=[O:16])[CH:13]=[C:12]([C:17]([O-:19])=[O:18])[O:11][C:10]=2[C:9]([CH2:20][CH2:21][CH3:22])=[C:8]2[C:3]=1[CH2:4][CH2:5][CH2:6][CH2:7]2.[Na+:27]

Participants

5

Reactant 3

HCID 65493ProxicromilHCID 516892Sodium BicarbonateHCID 5360545Sodium

Product 1

HCID 23668092HCID 23668092, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The product of step (a) (1.4 g) was suspended in water (20 ml) and sodium bicarbonate (356 mg) was added over 10 minutes. When homogeneity had been achieved the mixture was freeze-dried to yield a yellow solid which was shown to be a pure sample of the desired sodium salt (1.4 g; 93%).

Workup

  1. customwas freeze-dried
  2. customto yield a yellow solid which

Sources & evidence

ORD record
ord-af9d77c4f75e4f549a9535c7fc00e76c
Source dataset
uspto-grants-1979_06
Patent number
US04159273

Reaction notes

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