Potassium Carbonate → HCID 69201806, compound

HRID 2377290Notes

Reaction equation

HRID 2377290 reaction equation
[O:1]=[C:2]1[C:10]2[C:5](=[CH:6][CH:7]=[C:8]([CH2:11][N:12]3[CH2:17][CH2:16][N:15](C(OC(C)(C)C)=O)[CH2:14][CH2:13]3)[CH:9]=2)[CH2:4][CH2:3]1.C([O-])([O-])=O.[K+].[K+]>Cl>[N:12]1([CH2:11][C:8]2[CH:9]=[C:10]3[C:5]([CH2:4][CH2:3][C:2]3=[O:1])=[CH:6][CH:7]=2)[CH2:17][CH2:16][NH:15][CH2:14][CH2:13]1

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 69202467HCID 69202467, compound

Product 1

HCID 69201806HCID 69201806, compound

Reagents, catalysts & solvents 1

HCID 313Hydrochloric AcidSolvent

Procedure

A solution of Example 871A (0.83 g, 2.50 mmol) in 10% aqueous HCl (4 mL) was stirred at 60° C. for 15 min. The solution was brought to basic pH by the addition of K2CO3, then concentrated in vacuo to give a crude solid.

Workup

  1. concentrationconcentrated in vacuo
  2. customto give a crude solid

Sources & evidence

ORD record
ord-1cd0eb60981a47e0bace90b9835582f2
Source dataset
uspto-grants-2008_12
Patent number
US07468371B2

Reaction notes

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