2,4-Difluoroaniline → HCID 15230638, compound

HRID 2379466Notes

Reaction equation

HRID 2379466 reaction equation
[CH2:1]([N:13]1[N:17]=[N:16][C:15]([NH:18][C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)=[N:14]1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].ClC(Cl)(O[C:29](=[O:35])OC(Cl)(Cl)Cl)Cl.[F:37][C:38]1[CH:44]=[C:43]([F:45])[CH:42]=[CH:41][C:39]=1[NH2:40]>>[F:37][C:38]1[CH:44]=[C:43]([F:45])[CH:42]=[CH:41][C:39]=1[NH:40][C:29](=[O:35])[N:18]([C:15]1[N:16]=[N:17][N:13]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[N:14]=1)[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1

Participants

4

Reactant 3

HCID 97092,4-DifluoroanilineHCID 94429TriphosgeneHCID 10806269HCID 10806269, compound

Product 1

HCID 15230638HCID 15230638, compound

Procedure

In a manner similar to Example 1, 2-dodecyl-N-phenyl-2H-tetrazol-5-amine was reacted with triphosgene and 2,4-difluoroaniline to give the title compound, mp=55°-57° C.

Sources & evidence

ORD record
ord-354312747b784f4ebb4521363d11b9cb
Source dataset
uspto-grants-1994_11
Patent number
US05362744

Reaction notes

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