反应详情

In a 4 ounce glass jar were mixed 2-isocyanatoethyl methacrylate (15.5 g, 0.10 mol, available from Aldrich), 2-hydroxyethyl acrylate (11.6 g, 0.10 mol, available from Aldrich), and one drop of di-n-butyltin dilaurate (available from Alfa Aesar) to cause a slight exotherm. The jar was cooled briefly in an ice bath, and then left at room temperature overnight. NMR and IR spectral analyses confirmed the structure of the product.

1. temperatureThe jar was cooled briefly in an ice bath