反应详情

2-Methyl-4-nitro-1-pentafluoroethyl-benzene (2.55 g) was dissolved in CCl4 (30 ml) and AIBN (164 mg) and NBS (1.96 g) were added. The reaction was heated to reflux and stirred for 24 h. The mix was diluted with CH2Cl2, washed with sat'd NaHCO2, dried over MgSO4 and concentrated to give the compound as an oil which was used without further purification.

1. temperatureThe reaction was heated
2. temperatureto reflux
3. washwashed with sat'd NaHCO2
4. dry with materialdried over MgSO4
5. concentrationconcentrated